ESSENTIAL OIL OF CALENDULA OFFICINALIS
Abstract
The article presents the results of research into component composition of raw calendula’s essential oil. The study was conducted by gas chromatography mass spectrophotometry method under the following conditions: column - CP-Wax58FFAPCB24,5 mmx 250mm x0,20 mmnominal, the mobile-phase-He (helium), speed-column mobile phase-1.0 ml /min, volume sample injection-5mkl; resolutions(5:1), in the Split, high-boiling chamber -220 ◦C, detector temperature 275◦C; Aux-200 ◦ C, column temperature 70C◦ gradually increased from 10◦C / min to 250◦C, maintained to the end of analysis temperature regime(250◦C)for 5min.
In the course of the research the following substances were indentified - 1H cyclopropazulen-0, 981%, α-amorphous-1, 926%, γ-cadinene-11, 598%, 1H-cyclopropazulen 4-oldecahydro-1-0.825% viridiflorol-2, 029%, β-cubeb -3.809%, T-1 muurololnaftalenol-8.522%.
In addition, it was ascertained that in different parts of the world calendula’s essential oils differ from each other in qualitative composition and quantitative components.
References
Adler, G., Kasprzyk, Z. (1975). Free sterols, steryl esters, glucosides, acylated glucosides and water-soluble complexes in Calendula officinalis. Phytochemistry, 14 (3), 627-631. DOI: 10.1016/0031-9422(75)83006-8
Derkach, A.I., Komissarenko, N.F., & Chornobay, V.T. (1986). Kumarini sotsvetiy Calendula officinalis i Helichrysum arenarium [Coumarinin florescences Calendula officinalis and Helichrysum arenarium] International Journal Chemistry of Natural Compounds, 6, 777.
Gazim, Z.C., Rezende, C.M., Fraga, S.R., Dias, B.P., & et al. (2008). Analysis of the essential oils from Calendula officinalis growing in Brazil using three different extraction procedures. Revista Brasileira de Cikncias Farmackuticas Brazilian Journal of Pharmaceutical Sciences, 44 (3, jul./set). Retrieved from http://dx.doi.org/10.1590/S1516-93322008000300008
Gosudarstvennaya farmakopeya SSSR XI izd. (1990). vipusk 2. State Pharmacopoeia of the USSR XI ed. vypusk 2.(1990). No 2, 237. Retrieved from http://www.twirpx.com/file/165211/
Gracza, L. (1987). Oxygen-containing terpene derivatives from Calendula officinalis. Planta med., 53 (2), 227. DOI: 10.1055/s-2006-962683
Ivasenko, S.A., Pribytkova, L.N., Adekenov, S.M., Yushchenko, N.S., & Bondarec, V.G. (2000). Soderjanie karotinoidov i flavonoidov v sotsvetiyax nekotorix sortov Calendula officinalis L. [The content of carotenoids and flavonoids in thein florescence of some varieties of Calendula officinalis L.] Rast. Resources, 2, 107-110.
Ismagilov, R.R, Kostylev, D.A. (2000). Kalendula [Calendula]. Ufa, BGAU 102. Retrieved from http://ovoport.ru/calendula/kniga
Janiszowska, W., Rygier, J. (1985). Changes in the levels of prenylquinones and tocopherols in Calendula officinalis during vegetation. Physiol. Plantarum,. 63(4), 425-430. DOI: 10.1111/j.1399-3054.1985.tb02321.x
Janiszowska, W. (1987). Intracellular localization of tocopherol biosynthesis in Calendula officinalis. Phytochemistry, 26 (5), 1403-1407. DOI: 10.1016/S0031-9422(00)81822-1
Kasprzyk, Z., Janiszewska, W., & Sobszyk, A. (1973). Metabolism of a new series of oleanolic acid glucosides in Calendula officinalis shoots. Acta Biochim., 20 (3), 231-235. Retrieved from http://http://www.ncbi.nlm.nih.gov/pubmed/4749664
Konovalova, O.A, Ribalko, K.S. (1990). Biologicheski aktivnie veshestva Calendula officinalis L.[Biologically active substances of Calendula officinalis L.] Rast.. Resources, 26 (3), 448-463.
Ladygina, E.Y. (1992).Kalendula lekarstvennaya (Calendula officinalis L) [Calendula officinalis] Pharmacy ,40(4), 84-86. Retrieved from http://kgmu.kcn.ru:8888/cgi-bin/irbis64r_12/cgiirbis_64.exe?LNG=&Z21ID=&I21DBN=JOURNAL&P21DBN=JOURNAL&S21STN=1&S21REF=10&S21FMT=fullwebr&C21COM=S&S21CNR=20&S21P01=0&S21P02=1&S21P03=A=&S21STR=%D0%9B%D0%B0%D0%B4%D1%8B%D0%B3%D0%B8%D0%BD%D0%B0%20%D0%95.%20%D0%AF.
Marczal, G., Cserjesi, Z., Hethelyi, E., & Petri, G. (1987). Data on the essential oil content and composition of Calendula officinalis. Herba hung, 26 (2-3), 179-189. Retrieved from http// http://bazadan.com/book/ata-on-the-essential-oil-content-and-composition-of
Mashkovskii, M.D. (1998). Lekarstvennie sredstva [Lekarstvennye sredstva]. Izd.,12, 2, 433. Retrieved from http://www.webmedinfo.ru/lekarstvennye-sredstva-mashkovskij-m-d.html
Milborrow, B.V., Swift, I.E., & Netting, A.G. (1982). The stereochemistry of hydroxylation of the carotenoid lutein in Calendula officinalis. Phytochemistry, 21 (12), 2853-2857. DOI: 10.1016/0031-9422(80)85055-2
Pettit, G.R., Herald, Ch. L., Ode, R.H., Brown, P., Gust, D. J. & Michel, C. (1980). The isolation of loliolide from an Indian ocean opisthobranch mollusc. J. Natur. Product, 43 (6), 752-755. DOI: 10.1021/np50012a009
Peneva, P., Ivancheva, S., Vitkova, A., & Kozovska, V. (1985). Flavonoidi v Calendula officinalis [Flavonoids in Calendula officinalis]. Cropscience, 22 (4), 50-56.
Sharova, O.B. & Kurkin, V. A. (2007). Flavonoidi svetkov kalenduli lekarstvennoy [Flavonoids calendula officinalis flowers]. Journal Chemistry of plant raw materials,1, 65-68. Retrieved from http://www.chem.asu.ru/chemwood/volume11/2007_01/0701_065.pdf
Copyright information
- Authors retain copyright and grant the journal right of first publication with the work simultaneously licensed under a Creative Commons Attribution License (Creative Commons Attribution License 3.0 - CC BY 3.0) that allows others to share the work with an acknowledgement of the work's authorship and initial publication in this journal.
- Authors are able to enter into separate, additional contractual arrangements for the non-exclusive distribution of the journal's published version of the work (e.g., post it to an institutional repository or publish it in a book), with an acknowledgement of its initial publication in this journal.
- Authors are permitted and encouraged to post their work online (e.g., in institutional repositories or on their website) prior to and during the submission process, as it can lead to productive exchanges, as well as earlier and greater citation of published work (See The Effect of Open Access).
info@cbuni.cz, www.cbuni.cz, ojs.journals.cz